4-Fluorobenzoyl chloride → methyl N-(p-fluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
반응식
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:19])[O:17][CH3:18])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[F:20][C:21]1[CH:29]=[CH:28][C:24]([C:25](Cl)=[O:26])=[CH:23][CH:22]=1>>[F:20][C:21]1[CH:29]=[CH:28][C:24]([C:25]([N:19]=[C:16]([N:7]2[CH2:6][C:5]3[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=3[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8]2)[O:17][CH3:18])=[O:26])=[CH:23][CH:22]=1참가 물질
3
실험 절차
starting from methyl 5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate and p-fluorobenzoyl chloride, there is obtained methyl N-(p-fluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 136°-137.5° C.;
출처 및 근거
- ORD 기록
- ord-f7797218504c49249a891b77cd6318f7
- 출처 데이터셋
- uspto-grants-1991_05
- 특허 번호
- US05015640
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