Sulfuryl chloride → HCID 19834202, 화합물
반응식
[C:1]([O:4][C:5]1[CH:9]([CH3:10])[S:8][CH2:7][C:6]=1[C:11]([O:13][CH3:14])=[O:12])(=[O:3])[CH3:2].S(Cl)(Cl)(=O)=O>C(Cl)Cl>[C:1]([O:4][C:5]1[C:6]([C:11]([O:13][CH3:14])=[O:12])=[CH:7][S:8][C:9]=1[CH3:10])(=[O:3])[CH3:2]참가 물질
4
실험 절차
To methyl 4-acetoxy-2,5-dihydro-5-methyl-3-thiophene-carboxylate (68.3 g) in anhydrous methylene chloride (143 ml) was added sulphuryl chloride (30.4 ml) dropwise over 30 minutes. The black solution was stirred at room temperature over night.
출처 및 근거
- ORD 기록
- ord-282aca180c664b609aab2fd6f0db97c6
- 출처 데이터셋
- uspto-grants-1991_05
- 특허 번호
- US05015656
반응 노트
불러오는 중…