Butylamine → 2-Benzoyl-3-butylaminocrotononitrile
반응식
[C:1](/[C:9](=[C:12](/OC)\[CH3:13])/[C:10]#[N:11])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:16]([NH2:20])[CH2:17][CH2:18][CH3:19]>>[C:1](/[C:9](=[C:12](/[NH:20][CH2:16][CH2:17][CH2:18][CH3:19])\[CH3:13])/[C:10]#[N:11])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1참가 물질
3
실험 절차
A sample of 2.5 g. of 2-benzoyl-3-methoxycrotononitrile is dissolved in 10 ml. of n-butylamine. The solution is sealed in a stainless steel bomb and heated on a steam bath overnight. The bomb is then opened and the solvent evaporated under reduced pressure. A greenish oil is obtained which is distilled on a Kugelrohr apparatus at 200° C./0.1 mm. to obtain the yellow oily product.
후처리
- temperatureheated on a steam bath overnight
- customthe solvent evaporated under reduced pressure
- customA greenish oil is obtained which
- distillationis distilled on a Kugelrohr apparatus at 200° C./0.1 mm
- customto obtain the yellow oily product
출처 및 근거
- ORD 기록
- ord-ec7522ee6f3f4b73ace8ec19702a77dd
- 출처 데이터셋
- uspto-grants-1980_01
- 특허 번호
- US04181677
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