반응식
[CH2:1]([CH2:3][NH2:4])[OH:2].[ClH:5].[S:6]1(=[O:13])(=[O:12])[CH2:10][CH2:9][CH:8](N)[CH2:7]1>>[ClH:5].[OH:2][CH2:1][CH2:3][NH:4][CH:8]1[CH2:9][CH2:10][S:6](=[O:13])(=[O:12])[CH2:7]1참가 물질
3
실험 절차
The procedure of Example 1 was repeated substituting 95 percent monoethanolamine (28.6 parts) for the ammonium hydroxide of Example 1. A sticky solid was filtered after treatment with hydrochloric acid, and upon drying in vacuo over P2O5 weighed 59.6 g. (78.5 percent of theory) m.p. 122°-124° C.
후처리
- filtrationA sticky solid was filtered after treatment with hydrochloric acid
- dry with materialupon drying in vacuo over P2O5
출처 및 근거
- ORD 기록
- ord-5e6b7fafba8b41dcbb7a0b5e76c8f47e
- 출처 데이터셋
- uspto-grants-1980_01
- 특허 번호
- US04181806
연결된 노트
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