Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 3-Phenoxybenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 3-Phenoxybenzoyl chloride | HCID 2760341 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 3-Phenoxybenzamide | HCID 16618625 | — |
반응 단계
Saturated with anhydrous ammonia a solution containing 23 g (0.1 mole) of 3-phenoxybenzoyl chloride and 250 ml of AR chloroform. Continued stirring for 30 min., chilled to 0° and filtered. The product was pulverised, triturated in cold water and oven-dried to give 21.3 g, m.p. 127°-128°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04182881 |
| 출처 데이터셋 | uspto-grants-1980_01 |
| ORD ID | ord-a39fde958b4e4272b8722604470a7011 |
| 출처 메모 | uspto-grants-1980_01 |