Sodium Carbonate → N'-(3,4-dibromophenyl)-N,N,2-trimethylpropane-1,3-diamine

HRID 2052719노트

반응식

HRID 2052719 반응식
[Br:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[Br:9])[NH2:5].Cl.Cl[CH2:12][CH:13]([CH3:18])[CH2:14][N:15]([CH3:17])[CH3:16].C(=O)([O-])[O-].[Na+].[Na+]>C1(C)C=CC=CC=1>[Br:1][C:2]1[CH:3]=[C:4]([NH:5][CH2:12][CH:13]([CH3:18])[CH2:14][N:15]([CH3:17])[CH3:16])[CH:6]=[CH:7][C:8]=1[Br:9]

참가 물질

5

반응물 3

HCID 10340Sodium CarbonateHCID 5219813,4-DibromoanilineHCID 30838413-Chloro-2-methylpropyl(dimethyl)ammonium chloride

생성물 1

HCID 20376416N'-(3,4-dibromophenyl)-N,N,2-trimethylpropane-1,3-diamine

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

In the manner given in Example 5, 3,4-dibromoaniline, 3-chloro-2-methyl-1-dimethylaminopropane hydrochloride and sodium carbonate are heated in toluene to give N'-(3,4-dibromophenyl)-N,N,2-trimethylpropane-1,3-diamine.

출처 및 근거

ORD 기록
ord-9cdeab383b8d44c7b1d8d35d1d93968d
출처 데이터셋
uspto-grants-1980_01
특허 번호
US04186208

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