Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorine → HCID 178464806, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorine | HCID 24526 | — |
| 반응물 | Diisopropylethylamine | HCID 81531 | — |
| 반응물 | (2S)-2-(Diphenylmethyl)pyrrolidine | HCID 2734053 | — |
| 반응물 | HCID 178464831 | HCID 178464831 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | HCID 178464806 | HCID 178464806 | — |
반응 단계
Prepared analogously to Example 1d from rac.-2-chloro-4-{N-[1-(5-chloro-1H-benzimidazol-2-yl)ethyl]aminocarbonyl}benzoic acid, (2S)-2-benzhydrylpyrrolidine, PFTU, and diisopropylethylamine in DMSO at ambient temperature. HPLC-MS results: retention time: 5.18 minutes; C34H30Cl2N4O2 (597.54); mass spectrum: (M−H)−=597/599/601 (chlorine isotope).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07326791B2 |
| 출처 데이터셋 | uspto-grants-2008_02 |
| ORD ID | ord-428b05bbe09b46ca9a3891748a2c5f2b |
| 출처 메모 | uspto-grants-2008_02 |