Methanol → HCID 19364541, 화합물

반응식

C[Si](C)(C)[O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][NH:9][C:10](=[O:13])[CH:11]=[CH2:12].CO.C(C1C=C(C)C=C(C(C)(C)C)C=1O)(C)(C)C>C(O)(=O)C>[OH:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][NH:9][C:10](=[O:13])[CH:11]=[CH2:12]

참가 물질

실험 절차

N-[2-(2-trimethylsiloxyethoxy)ethyl]acrylamide (73.5 g), methanol (400 g) and acetic acid (50 g) were introduced into a 1 L eggplant type flask and were mixed to a homogeneous state, after which the mixture was allowed to stand at room temperature overnight. 2,6-di-t-butyl-4-methylphenol (0.2 g) was added, after which the solvent was removed by means of a rotary vacuum evaporator (using a vacuum pump; bath temperature, 60 to 70° C.). The volatile components were removed by means of a vacuum pump under decreased pressure over a two-hour period at 70° C. and N-[2-(2-hydroxyethoxy)ethyl]acrylamide was obtained as a yellow transparent, viscous liquid.