p-Bromobenzenesulfonyl chloride → HCID 178484844, 화합물

HRID 2057224

반응식

HRID 2057224 반응식
[CH3:1][NH:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([OH:9])[CH2:5][CH2:4]1.[Br:10][C:11]1[CH:16]=[CH:15][C:14]([S:17](Cl)(=[O:19])=[O:18])=[CH:13][CH:12]=1>>[Br:10][C:11]1[CH:16]=[CH:15][C:14]([S:17]([N:2]([C@H:3]2[CH2:8][CH2:7][C@H:6]([OH:9])[CH2:5][CH2:4]2)[CH3:1])(=[O:19])=[O:18])=[CH:13][CH:12]=1

참가 물질

3

반응물 2

HCID 7396p-Bromobenzenesulfonyl chlorideHCID 178484843HCID 178484843, 화합물

생성물 1

HCID 178484844HCID 178484844, 화합물

실험 절차

In analogy to example 11.9D. trans-4-Methylamino-cyclohexanol and 4-bromobenzenesulfonylchloride were reacted to yield trans-4-Bromo-N-(4-hydroxy-cyclohexyl)-N-methyl-benzenesulfonamide as off-white solid, MS: 348 (MH+, 1Br).

출처 및 근거

ORD 기록
ord-f4898dbbecdd42239493a5e15dc1940e
출처 데이터셋
uspto-grants-2008_02
특허 번호
US07335687B2

연결된 노트

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