1,3-Dibromopropane → HCID 178484846, 화합물

HRID 2057226

반응식

HRID 2057226 반응식
[OH:1][C@H:2]1[CH2:7][CH2:6][C@H:5]([N:8]([CH3:22])[S:9]([C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:20])[F:19])=[CH:14][CH:13]=2)(=[O:11])=[O:10])[CH2:4][CH2:3]1.[Br:23][CH2:24][CH2:25][CH2:26]Br>>[Br:23][CH2:24][CH2:25][CH2:26][O:1][C@H:2]1[CH2:7][CH2:6][C@H:5]([N:8]([CH3:22])[S:9]([C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:19])[F:20])=[CH:14][CH:13]=2)(=[O:11])=[O:10])[CH2:4][CH2:3]1

참가 물질

3

반응물 2

HCID 80011,3-DibromopropaneHCID 178484845HCID 178484845, 화합물

생성물 1

HCID 178484846HCID 178484846, 화합물

실험 절차

In analogy to example 11.11, trans-N-(4-Hydroxy-cyclohexyl)-N-methyl-4-trifluoromethyl-benzenesulfonamide and 1,3-dibrompropane were converted to yield trans-N-[4-(3-Bromo-propoxy)-cyclohexyl]-N-methyl-4-trifluoromethyl-benzenesulfonamide as off-white semisolid, MS: 320 [M−C3H6BrO].

출처 및 근거

ORD 기록
ord-7697de97d5f6461e919602a2572ba4e4
출처 데이터셋
uspto-grants-2008_02
특허 번호
US07335687B2

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