Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 9,10-Anthracenedicarboxaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 9,10-Dihydro-9,10-anthracenedicarboxaldehyde | HCID 11230096 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 9,10-Anthracenedicarboxaldehyde | HCID 81500 | — |
반응 단계
To a solution of 240 mg. of the product of Example 2 (prepared as described) in 15 ml. of acetonitrile is added a solution of 0.30 ml. of triethylamine in 5 ml. of acetonitrile. The reaction mixture is stirred at room temperature for 4 hours then is cooled in an ice bath. The precipitate is collected by filtration to give 136 mg. of the desired crude product as orange crystals, mp. 224°-228° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04211726 |
| 출처 데이터셋 | uspto-grants-1980_07 |
| ORD ID | ord-a8c2e8a12ed643ba857366931310ed63 |
| 출처 메모 | uspto-grants-1980_07 |