N1-(5-chloro-2-methoxy-4-nitrophenyl)acetamide → 5-Chloro-2-methoxy-4-nitroaniline
반응식
C([NH:4][C:5]1[CH:10]=[C:9]([Cl:11])[C:8]([N+:12]([O-:14])=[O:13])=[CH:7][C:6]=1[O:15][CH3:16])(=O)C>[OH-].[K+]>[NH2:4][C:5]1[CH:10]=[C:9]([Cl:11])[C:8]([N+:12]([O-:14])=[O:13])=[CH:7][C:6]=1[O:15][CH3:16]참가 물질
3
실험 절차
0.5 mol (99.5 g) of 2-acetamido-4-chloro-5-nitroanisole and 125 ml of a solution of potassium hydroxide (140 g of KOH/100 ml of water) are introduced into a 500 ml flask; the mixture is brought to between 100° and 110° C. for one hour and three quarters; the product is dried without heating and washed with water.
후처리
- customthe product is dried
- temperaturewithout heating
- washwashed with water
출처 및 근거
- ORD 기록
- ord-c6dbbc4a161a46cb97be7a9cb9ce295a
- 출처 데이터셋
- uspto-grants-1980_07
- 특허 번호
- US04211776
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