Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromine → 3-(4-Bromophenoxy)benzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| 생성물 | 3-(4-Bromophenoxy)benzaldehyde | HCID 12874363 | — |
반응 단계
9.60 Grams (0.060 mole) of bromine were added dropwise to 9.90 g (0.050 mole) of m-phenoxybenzaldehyde at 0° C. taking a period of 1 hour with vigorous stirring. After the addition was finished, the reaction was continued for a further 3 hours at the same temperature. The unreacted bromine was distilled off under reduced pressure from the reaction system to obtain m-(p-bromophenoxy)benzaldehyde (No. 9 in Table 2).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04212829 |
| 출처 데이터셋 | uspto-grants-1980_07 |
| ORD ID | ord-35a8d702604542d990f26c113d0cf7fe |
| 출처 메모 | uspto-grants-1980_07 |