참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium Chlorate | HCID 516902 | — |
| 반응물 | Echinenone | HCID 5281236 | — |
| 촉매 | Iodine | HCID 807 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Canthaxanthin | HCID 5281227 | 65.3% |
반응 단계
100 mg of echinenone are dissolved in 10 ml of chloroform under a nitrogen atmosphere and are oxidized with 100 mg of sodium chlorate in 1 ml of water after having added 2 mg of iodine dissolved in 1 ml of chloroform. After stirring for 24 hours at -20° C., 67 mg of canthaxanthin having an all-trans content of 81% are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04212827 |
|---|
| 출처 데이터셋 | uspto-grants-1980_07 |
|---|
| ORD ID | ord-648c87607f584ecda96f203161e74617 |
|---|
| 출처 메모 | uspto-grants-1980_07 |
|---|
