Sodium Carbonate Decahydrate → Pentabromodiphenyl ethers

HRID 2058053

반응식

HRID 2058053 반응식
[CH:1]1[C:6]([Br:7])=[CH:5][C:4]([Br:8])=[C:3]([O:9][C:10]2[C:15]([Br:16])=[CH:14][C:13]([Br:17])=[C:12]([Br:18])[CH:11]=2)[CH:2]=1.P(OC1C=CC=CC=1)(OC1C=CC=CC=1)(OCC(CC)CCCC)=O.O.O.O.O.O.O.O.O.O.O.C(=O)([O-])[O-].[Na+].[Na+]>O>[CH:1]1[C:6]([Br:7])=[CH:5][C:4]([Br:8])=[C:3]([O:9][C:10]2[C:15]([Br:16])=[CH:14][C:13]([Br:17])=[C:12]([Br:18])[CH:11]=2)[CH:2]=1

참가 물질

4

반응물 2

HCID 151402Sodium Carbonate DecahydrateHCID 131711832HCID 131711832, 화합물

생성물 1

HCID 36159Pentabromodiphenyl ethers

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Using the procedure of Examples II and IV, the pentabromodiphenyl ether-2-ethylhexyl diphenyl phosphate blend was heated to 130° C., and sodium carbonate decahydrate (2.7% W/W on the blend) was added and subjected to agitation in the closed system for one-half hour. Thereafter, the system was opened in order to permit water to escape. The molten mixture was filtered to obtain the purified blend. Relevant properties of the blend are given in Table III.

후처리

  1. waitsubjected to agitation in the closed system for one-half hour
  2. filtrationThe molten mixture was filtered
  3. customto obtain the purified blend

출처 및 근거

ORD 기록
ord-e3755f6f64ff4cec9d58fbca0c3ac339
출처 데이터셋
uspto-grants-1980_07
특허 번호
US04214103

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