Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Fumaric Acid → 1-Cyclooctylmethylimidazole hydrogen fumarate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Fumaric Acid | HCID 444972 | — |
| 반응물 | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Cyclooctylmethylimidazole hydrogen fumarate | HCID 20550237 | 71.9% |
반응 단계
A solution of fumaric acid (0.22 g) in hot ethanol (10 ml) was added to a solution of 1 -cyclooctylmethyl imidazole (0.38 g) in ethanol (4 ml). After boiling for 10 minutes the solution was evaporated to afford a white solid. Recrystallisation from ethyl acetate afforded 1-cyclooctylmethylimidazole hydrogen fumarate (0.42 g) as white needles, m.p. 147° to 148° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04317830 |
| 출처 데이터셋 | uspto-grants-1982_03 |
| ORD ID | ord-e96747ec888f4ddc9acd75a8341803fe |
| 출처 메모 | uspto-grants-1982_03 |