Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalic Acid → 1-Cyclooctylmethylimidazole oxalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalic Acid | HCID 971 | — |
| 반응물 | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Cyclooctylmethylimidazole oxalate | HCID 20550257 | — |
반응 단계
A solution of oxalic acid (0.17 g) and 1-cyclooctylmethylimidazole (0.38 g) in ethanol (20 ml) was boiled for 0.25 hour, when evaporation of the solution afforded a white solid. Recrystallisation of the solid from ethyl acetate/ethanol/petroleum ether (b.p. 40°-60°) afforded 1-cyclooctylmethylimidazole oxalate as white needles, m.p. 141°-142° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04317830 |
| 출처 데이터셋 | uspto-grants-1982_03 |
| ORD ID | ord-70472e86af664ee2988076d777f95df2 |
| 출처 메모 | uspto-grants-1982_03 |