Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Phenylprop-2-En-1-Ol → (3-Phenyl-2-propenyl)-2-hydroxy-3-methylbenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Phenylprop-2-En-1-Ol | HCID 308 | — |
| 반응물 | Phosphoric Acid | HCID 1004 | — |
| 반응물 | 3-Methylsalicylic Acid | HCID 6738 | — |
| 생성물 | (3-Phenyl-2-propenyl)-2-hydroxy-3-methylbenzoate | HCID 53972063 | 89.1% |
반응 단계
Using the method of example 1, 15.24 g of 2-hydroxy-3-methylbenzoic acid (0.1 moles), 40.251 g of 3-phenyl-2-propen-1-ol (0.3 moles) of 4.9 g of anhydrous phosphoric acid (0.05 moles) give 23.9 g (yield 89%) of (3-phenyl-2-propenyl)-2-hydroxy-3-methylbenzoate, m.p. 154°-154.5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04317917 |
| 출처 데이터셋 | uspto-grants-1982_03 |
| ORD ID | ord-5506c82df35e45fdb6bb7a935ff9399e |
| 출처 메모 | uspto-grants-1982_03 |