Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylammonium chloride → 3-Benzylaminoacrylonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylammonium chloride | HCID 2724127 | — |
| 반응물 | Sodium 3-hydroxyacrylonitrile | HCID 86738287 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 3-Benzylaminoacrylonitrile | HCID 70548701 | 57.1% |
반응 단계
32.5 g (0.25 mol) of sodium-3-hydroxyacrylonitrile (content 70%) and 43.1 g (0.3 mol) of benzylamine hydrochloride are refluxed for 5 h in 150 ml of acetonitrile. After removal of the solid by filtration and withdrawal of the solvent, the product was dissolved in chloroform and washed with water. Subsequent vacuum distillation yielded 22.6 g of 3-benzylaminoacrylonitrile (57.1%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04319024 |
| 출처 데이터셋 | uspto-grants-1982_03 |
| ORD ID | ord-0f57112ce6d9455cb4c8af2ad9496e10 |
| 출처 메모 | uspto-grants-1982_03 |