Benzene → HCID 12962346, 화합물
반응식
C1C=CC=CC=1.[Cl:7][C:8]1[CH:13]=[CH:12][C:11]([CH:14]2[NH:18][CH2:17][CH2:16][O:15]2)=[CH:10][CH:9]=1.[Cl:19][CH:20]([Cl:24])[C:21](Cl)=[O:22]>C(N(CC)CC)C>[Cl:7][C:8]1[CH:9]=[CH:10][C:11]([CH:14]2[N:18]([C:21](=[O:22])[CH:20]([Cl:24])[Cl:19])[CH2:17][CH2:16][O:15]2)=[CH:12][CH:13]=1참가 물질
5
실험 절차
Twenty-two (22) ml. of a benzene solution containing 5.5 g. of 2-p-chlorophenyl oxazolidine was mixed with 25 ml. of benzene and 3.1 g. of triethylamine and stirred at room temperature, while 4.4 g. of dichloroacetyl chloride was added dropwise. The mixture was allowed to stand for about 30 minutes, washed with water, separated, dried over magnesium sulfate and then stripped. There was obtained a yield of 3.4 g. of an oil, the title compound, ND30 =1.5668.
후처리
- washwashed with water
- customseparated
- dry with materialdried over magnesium sulfate
- customThere was obtained a yield of 3.4 g
출처 및 근거
- ORD 기록
- ord-de58138edee74bb19d6239455ecd5861
- 출처 데이터셋
- uspto-grants-1982_03
- 특허 번호
- US04322240
반응 노트
불러오는 중…