Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dimethoxybenzoyl chloride → 2,6-Dimethoxy-N-(4-(4-(trifluoromethyl)phenyl)-5-isoxazolyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dimethoxybenzoyl chloride | HCID 74810 | — |
| 반응물 | 4-(4-(Trifluoromethyl)phenyl)-5-aminoisoxazole | HCID 20546740 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2,6-Dimethoxy-N-(4-(4-(trifluoromethyl)phenyl)-5-isoxazolyl)benzamide | HCID 13035564 | — |
반응 단계
4-(4-(Trifluoromethyl)phenyl)-5-aminoisoxazole (1.0 g) and 2,6-dimethoxybenzoylchloride (2 g) were refluxed in 100 ml. toluene for 3 hours. The reaction mixture was cooled and the final product was then collected and recrystallized from ethanol, m.p. 199°-201° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04322429 |
| 출처 데이터셋 | uspto-grants-1982_03 |
| ORD ID | ord-680c61f813ff4726bed668b4b9331c3a |
| 출처 메모 | uspto-grants-1982_03 |