6-Chloro-3-pyridinecarbonitrile → HCID 59401349, 화합물

HRID 2060866노트

반응식

HRID 2060866 반응식
[OH:1][CH2:2][C:3]1[CH:12]=[CH:11][CH:10]=[C:9]2[C:4]=1[CH:5]=[CH:6][CH:7]=[C:8]2[OH:13].Cl[C:15]1[CH:22]=[CH:21][C:18]([C:19]#[N:20])=[CH:17][N:16]=1>>[OH:1][CH2:2][C:3]1[CH:12]=[CH:11][CH:10]=[C:9]2[C:4]=1[CH:5]=[CH:6][CH:7]=[C:8]2[O:13][C:15]1[CH:22]=[CH:21][C:18]([C:19]#[N:20])=[CH:17][N:16]=1

참가 물질

3

반응물 2

HCID 51520946-Chloro-3-pyridinecarbonitrileHCID 57979480HCID 57979480, 화합물

생성물 1

HCID 59401349HCID 59401349, 화합물

실험 절차

Using the procedure outlined in Preparation 15, 5-hydroxymethylnaphthalen-1-ol (Preparation 32) and 6-chloronicotinonitrile were converted to the title compound: RT=3.17 min; m/z (ES+)=277.1 [M+H]+.

출처 및 근거

ORD 기록
ord-8059c07751a94e15add25ebc96c457f5
출처 데이터셋
uspto-grants-2012_10
특허 번호
US08278442B2

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