6-Chloro-3-pyridinecarbonitrile → HCID 68470136, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:12]=[CH:11][CH:10]=[C:9]2[C:4]=1[CH:5]=[CH:6][CH:7]=[C:8]2[CH2:13][N:14]([CH2:20][CH2:21][CH:22]([CH3:24])[CH3:23])[CH2:15][CH2:16][CH:17]([CH3:19])[CH3:18].ClC1[CH:31]=[CH:30][C:29]([C:32]#[N:33])=[CH:28][N:27]=1>>[CH3:23][CH:22]([CH3:24])[CH2:21][CH2:20][N:14]([CH2:13][C:8]1[CH:7]=[CH:6][CH:5]=[C:4]2[C:9]=1[CH:10]=[CH:11][CH:12]=[C:3]2[O:2][C:1]1[CH:31]=[CH:30][C:29]([C:32]#[N:33])=[CH:28][N:27]=1)[CH2:15][CH2:16][CH:17]([CH3:18])[CH3:19]

참가 물질

반응물 2

HCID 51520946-Chloro-3-pyridinecarbonitrile

HCID 68466114HCID 68466114, 화합물

생성물 1

HCID 68470136HCID 68470136, 화합물

실험 절차

Using the procedure outlined in Preparation 14 and Preparation 15, (5-methoxynaphthalen-1-ylmethyl)-bis-(3-methylbutyl)amine (Preparation 29) and 2-chloro-5-cyanopyridine were converted to the title compound: RT=2.93 min; m/z (ES+)=416.8 [M+H]+.

출처 및 근거

ORD 기록: ord-6940b8d5ffcd4705abb3de8ea5217ffe
출처 데이터셋: uspto-grants-2012_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08278442B2

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