Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2,3-Propanetricarboxylic acid → Tricarballylic acid tris(2-methylcyclohexylamide)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2,3-Propanetricarboxylic acid | HCID 14925 | — |
| 반응물 | 2-Methylcyclohexylamine | HCID 23432 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | Tricarballylic acid tris(2-methylcyclohexylamide) | HCID 66687139 | — |
반응 단계
Next, 3.52 g (20 mmol) of 1,2,3-propanetricarboxylic acid (made by Nacalai Tesque) and 13.6 g (120 mmol) of 2-methylcyclohexylamine were added to the xylene solution of a tricresol boric acid ester obtained above, and the contents were refluxed under heating and reacted for 3 hours. This gave a crude 1,2,3-propanetricarboxylic acid tris(2-methylcyclohexylamide) as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07745661B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-ecb61f148f9b42ad9efdb3b2bf48368c |
| 출처 메모 | uspto-grants-2010_06 |