Potassium Nitrate → HCID 178513826, 화합물
반응식
[OH:1][C:2]1[C:3]([C:8]([NH2:10])=[O:9])=[N:4][CH:5]=[CH:6][N:7]=1.[N+:11]([O-])([O-:13])=[O:12].[K+]>S(=O)(=O)(O)O.O>[OH:1][C:2]1[C:3]([C:8]([NH2:10])=[O:9])=[N:4][C:5]([N+:11]([O-:13])=[O:12])=[CH:6][N:7]=1참가 물질
5
반응 조건
- 온도
- 40 °C
실험 절차
In 24 mL of concentrated sulfuric acid is suspended 4.00 g of 3-hydroxy-2-pyrazinecarboxamide. To the suspension is added 3.09 g of potassium nitrate under ice-cooling. The resulting mixture is stirred at 40° C. for 3 hours. The reaction mixture is poured into 240 mL of water, and the deposited crystals are collected by filtration. The crystals thus obtained are suspended in 80 mL of water and heated under reflux for 30 minutes. After cooling, the crystals are collected by filtration to obtain 2.45 g of 3-hydroxy-6-nitro-2-pyrazinecarboxamide.
후처리
- temperaturecooling
- filtrationthe deposited crystals are collected by filtration
- customThe crystals thus obtained
- temperatureheated
- temperatureunder reflux for 30 minutes
- temperatureAfter cooling
- filtrationthe crystals are collected by filtration
출처 및 근거
- ORD 기록
- ord-d95554f558404ca4a7162380e1809bbf
- 출처 데이터셋
- uspto-grants-2012_10
- 특허 번호
- USRE043748E1
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