Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-METHYLACETOPHENONE → N-(1-p-Tolyl-ethylidene)-N'-(2-trifluoromethyl-quinazolin-4-yl)-hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-METHYLACETOPHENONE | HCID 8500 | — |
| 반응물 | 4-Hydrazino-2-(trifluoromethyl)quinazoline | HCID 1475464 | — |
| 생성물 | N-(1-p-Tolyl-ethylidene)-N'-(2-trifluoromethyl-quinazolin-4-yl)-hydrazine | HCID 84890440 | — |
반응 단계
The title compound was prepared from (2-trifluoromethyl-quinazolin-4-yl)-hydrazine (250 mg, 1.1 mmol) and 4′-methylacetophenone (0.22 mL, 1.6 mmol) by a procedure similar to Example 1, step 4 yielding 225 mg (60%) of a yellow solid. HPLC Purity: 95%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08288398B2 |
| 출처 데이터셋 | uspto-grants-2012_10 |
| ORD ID | ord-11c0bab9bdb44b1396a859d1e188a678 |
| 출처 메모 | uspto-grants-2012_10 |