Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
P-Chloroacetophenone → N-[1-(4-Chloro-phenyl)ethylidene]-N'-(2-methyl-6-phenyl-pyrimidin-4-yl)-hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | P-Chloroacetophenone | HCID 7467 | — |
| 반응물 | 4-Hydrazinyl-2-methyl-6-phenylpyrimidine | HCID 824627 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-[1-(4-Chloro-phenyl)ethylidene]-N'-(2-methyl-6-phenyl-pyrimidin-4-yl)-hydrazine | HCID 73320073 | — |
반응 단계
The title compound was prepared from 4-hydrazino-2-methyl-6-phenylpyrimidine (300 mg, 1.5 mmol) and 1-(4-Chloro-phenyl)-ethanone (136 μL, 1.05 mmol) in 8.0 mL of ethanol by a procedure similar to example 1, step 4 yielding 190 mg (38%) of an off-white solid. HPLC Purity: 98%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08288398B2 |
| 출처 데이터셋 | uspto-grants-2012_10 |
| ORD ID | ord-c4452f54b6634401ab1e7eb9b7cb1496 |
| 출처 메모 | uspto-grants-2012_10 |