Cyclopropylmethyl methanesulfonate → HCID 60911320, 화합물

반응식

[NH2:1][C:2]1[N:6]=[CH:5][NH:4][N:3]=1.[CH:7]1([CH2:10]OS(C)(=O)=O)[CH2:9][CH2:8]1>>[CH:7]1([CH2:10][N:4]2[CH:5]=[N:6][C:2]([NH2:1])=[N:3]2)[CH2:9][CH2:8]1

참가 물질

반응물 2

HCID 135444Cyclopropylmethyl methanesulfonate

HCID 178418311HCID 178418311, 화합물

생성물 1

HCID 60911320HCID 60911320, 화합물

실험 절차

Prepared in analogy to example 3a) starting with 3-amino-1,2,4-triazole and methanesulfonic acid cyclopropylmethyl ester (Journal of the American Chemical Society 128, 3118 (2006)). The title compound was obtained as a brownish solid (Yield=25%). MS ISP (m/e): 138.1 (100) [M+].

후처리

customPrepared in analogy to example 3a)

출처 및 근거

ORD 기록: ord-e5494ec18c3a47b9a36ca3e36441a0c7
출처 데이터셋: uspto-grants-2012_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08288403B2

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