HCID 7019333, 화합물 → HCID 46216255, 화합물

HRID 2063665노트

반응식

HRID 2063665 반응식
Br[C:2]1[CH:3]=[CH:4][C:5]([N:10]2[CH:14]=[C:13]([CH3:15])[N:12]=[CH:11]2)=[C:6]([CH:9]=1)[C:7]#[N:8].[CH3:16][C:17]1[CH:29]=[CH:28][C:20]([CH2:21][N:22]2[CH:26]=[N:25][C:24]([NH2:27])=[N:23]2)=[CH:19][CH:18]=1>>[CH3:16][C:17]1[CH:18]=[CH:19][C:20]([CH2:21][N:22]2[CH:26]=[N:25][C:24]([NH:27][C:2]3[CH:3]=[CH:4][C:5]([N:10]4[CH:14]=[C:13]([CH3:15])[N:12]=[CH:11]4)=[C:6]([CH:9]=3)[C:7]#[N:8])=[N:23]2)=[CH:28][CH:29]=1

참가 물질

3

반응물 2

HCID 7019333HCID 7019333, 화합물HCID 669615175-bromo-2-(4-methyl-1H-imidazol-1-yl)benzonitrile

생성물 1

HCID 46216255HCID 46216255, 화합물

실험 절차

Prepared in analogy to example 1b) starting with 5-bromo-2-(4-methyl-imidazol-1-yl)-benzonitrile and 1-(4-methyl-benzyl)-1H-[1,2,4]triazol-3-ylamine. The title compound was obtained as a white solid (Yield=50%). MS ISP (m/e): 370.1 (100) [(M+H)+].

후처리

  1. customPrepared in analogy to example 1b)

출처 및 근거

ORD 기록
ord-18c03d10a69e4ea9a015e006905df372
출처 데이터셋
uspto-grants-2012_10
특허 번호
US08288403B2

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