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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2064571생성일: 2026년 10월 25일

1H-Indazol-3-ylmethanol → HCID 178520025, 화합물

https://huagongshe.com/reaction/2064571

반응식

참여 물질

역할이름HCID투입량
반응물1H-Indazol-3-ylmethanolHCID 178520026—
촉매HCID 178418406HCID 178418406—
용매1,2-DimethoxyethaneHCID 8071—
생성물HCID 178520025HCID 17852002590.2%

반응 조건

온도20 °C

반응 단계

A solution of 2.27 g of (1H-indazol-3-yl)methanol in 220 ml of 1,2-dimethoxyethane is added to 13.32 g of manganese dioxide. After one hour at a temperature in the region of 20° C., the reaction mixture is refluxed for 15 minutes. After cooling to a temperature in the region of 20° C., the reaction medium is filtered through a sinter funnel packed with Celite. The collected filtrate is concentrated under reduced pressure at a temperature in the region of 40° C. 2.02 g of 1H-indazole-3-carboxaldehyde are thus obtained in the form of a yellow powder, the characteristics of which are as follows:

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08288425B2
출처 데이터셋uspto-grants-2012_10
ORD IDord-92e718e1225b4f5b84e6107ab8c77e91
출처 메모uspto-grants-2012_10