Methoxyacetic Acid → 2-Methoxymethyl-5-phenyl-oxazole-4-carboxylic acid

HRID 2065092노트

반응식

[CH:1]1[CH:6]=[CH:5][C:4]([CH:7]([OH:13])[CH:8]([NH2:12])[C:9]([OH:11])=[O:10])=[CH:3][CH:2]=1.[CH3:14][O:15][CH2:16][C:17](O)=O>>[CH3:14][O:15][CH2:16][C:17]1[O:13][C:7]([C:4]2[CH:3]=[CH:2][CH:1]=[CH:6][CH:5]=2)=[C:8]([C:9]([OH:11])=[O:10])[N:12]=1

참가 물질

반응물 2

HCID 12251Methoxyacetic Acid

HCID 94134DL-Phenylserine

생성물 1

HCID 669285712-Methoxymethyl-5-phenyl-oxazole-4-carboxylic acid

실험 절차

Prepared starting from DL-3-phenylserine hydrate following sequentially general procedures Y, Z with methoxyacetic acid, Z1 and Z2. LC-MS-conditions 02: tR=0.81 min; [M+H]+=234.45.

후처리

customPrepared

출처 및 근거

ORD 기록: ord-09a54b2e70494939a8fd1dcdec6c97cd
출처 데이터셋: uspto-grants-2012_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08288419B2

반응 노트

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