Toluene → HCID 86607702, 화합물
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Br[C:2]1[CH:3]=[C:4]([CH2:15][C:16]([O-:18])=[O:17])[CH:5]=[CH:6][C:7]=1[O:8][CH2:9][O:10][CH2:11][CH2:12][O:13][CH3:14].[CH3:19][O:20][CH2:21][CH2:22][O:23][CH2:24][O:25][C:26]1[C:33](B2OC(C)(C)C(C)(C)O2)=[CH:32][CH:31]=[CH:30][C:27]=1[CH:28]=[O:29].[C:43]1(C)C=CC=CC=1>>[CH3:43][O:18][C:16](=[O:17])[CH2:15][C:4]1[CH:3]=[C:2]([C:33]2[CH:32]=[CH:31][CH:30]=[C:27]([CH:28]=[O:29])[C:26]=2[O:25][CH2:24][O:23][CH2:22][CH2:21][O:20][CH3:19])[C:7]([O:8][CH2:9][O:10][CH2:11][CH2:12][O:13][CH3:14])=[CH:6][CH:5]=1참가 물질
4
실험 절차
Proceeding as in Reference 19, but substituting 3-bromo-4-(2-methoxyethoxymethoxy)phenylacetate (2.43 g, 7.28 mmol) and 2-(2-methoxyethoxymethoxy)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzaldehyde in toluene (7.28 mmol, 0.1 M, 73 mL), gave methyl[3′-formyl-6,2′-bis(2-methoxyethoxymethoxy)biphenyl-3-yl]acetate (2.42 g).
출처 및 근거
- ORD 기록
- ord-f2a3bcd1f6d248059b8f981610cfeee0
- 출처 데이터셋
- uspto-grants-2012_10