Boc aminomethyl bromide → 3-(Dimethylamino)-5-(prop-1-en-2-yl)benzonitrile

HRID 2070940노트

반응식

HRID 2070940 반응식
Br[C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([N:10]([CH3:12])[CH3:11])[CH:9]=1)[C:5]#[N:6].C(NCBr)(O[C:16](C)([CH3:18])[CH3:17])=O>>[CH3:11][N:10]([CH3:12])[C:8]1[CH:7]=[C:4]([CH:3]=[C:2]([C:16]([CH3:18])=[CH2:17])[CH:9]=1)[C:5]#[N:6]

참가 물질

3

반응물 2

HCID 20614913Boc aminomethyl bromideHCID 686703103-Bromo-5-(dimethylamino)benzonitrile

생성물 1

HCID 686699313-(Dimethylamino)-5-(prop-1-en-2-yl)benzonitrile

실험 절차

3-(dimethylamino)-5-(prop-1-en-2-yl)benzonitrile was synthesized from 3-bromo-5-(dimethylamino)benzonitrile following the general procedure as described for the Cbz protected Boc aminomethyl bromide.

출처 및 근거

ORD 기록
ord-98e6e4c0f9b64234a628a4918415f514
출처 데이터셋
uspto-grants-2012_10
특허 번호
US08299267B2

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