Pyridine → HCID 21409997, 화합물

HRID 2071918

반응식

HRID 2071918 반응식
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH2:15][C:16]([F:24])([F:23])[CH:17]([F:22])[C:18]([F:21])([F:20])[F:19])=[O:13].[N:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>CO>[Br-:1].[N:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH2:15][C:16]([F:24])([F:23])[CH:17]([F:22])[C:18]([F:21])([F:20])[F:19])=[O:13]

참가 물질

4

반응물 2

HCID 1049PyridineHCID 214099962,2,3,4,4,4-Hexafluorobutyl 11-bromoundecylate

생성물 1

HCID 21409997HCID 21409997, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The process of producing the surfactant of claim 1 comprising (a) reacting at reflux 2,2,3,4,4,4-hexafluorobutanol and 11-bromoundecanoic acid in presence of methane sulfonic acid as a catalyst and benzene as a solvent to obtain 2,2,3,4,4,4-hexafluorobutyl 11-bromoundecylate and then (b) reacting at reflux 2,2,3,4,4,4-hexafluorobutyl 11-bromoundecylate with pyridine in presence of methanol as a solvent to obtain 2,2,3,4,4,4-hexafluorobutyl 11-pyridylundecylate bromide.

출처 및 근거

ORD 기록
ord-8486ada63155495d8c3a4f1b0de6f8e9
출처 데이터셋
uspto-grants-1977_09
특허 번호
US04049668

연결된 노트

불러오는 중…