참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,2-Dichlorobenzene | HCID 7239 | — |
| 반응물 | 1,1,2,3,3,3-Hexachloro-1-propene | HCID 15902 | — |
| 반응물 | Tetrachloroethylene | HCID 31373 | — |
| 생성물 | Hexachloroindene | HCID 53971155 | 48.7% |
반응 단계
A mixture containing 29.4 grams (0.2 mole), of ortho-dichlorobenzene, 50 grams (0.2 moles) of hexachloropropylene and 2.5 grams of ferric chloride in 250 milliliters of perchloroethylene was heated and stirred by the process of Example I for about 4 hours at reflux (125° C.). The reaction mixture was then washed with concentrated hydrochloric acid, then water and distilled to give a 48.7% yield of hexachloroindene. The product was confirmed by infrared and NMR spectra analysis as structured.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04049727 |
|---|
| 출처 데이터셋 | uspto-grants-1977_09 |
|---|
| ORD ID | ord-ebe79f31ccfc476ca69a935b53df9376 |
|---|
| 출처 메모 | uspto-grants-1977_09 |
|---|
