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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2072279생성일: 2026년 10월 25일

Pyridine → 1-Amino-2,4-di-n-dodecylaminoanthraquinone

https://huagongshe.com/reaction/2072279

반응식

참여 물질

역할이름HCID투입량
반응물PyridineHCID 1049—
반응물1-Amino-2,4-dibromoanthraquinoneHCID 6681—
반응물DodecylamineHCID 13583—
반응물Potassium AcetateHCID 517044—
촉매Cupric acetateHCID 8895—
용매BenzeneHCID 241—
생성물1-Amino-2,4-di-n-dodecylaminoanthraquinoneHCID 21407063—

반응 단계

A reactor was charged with 19 g of 1-amino-2,4-dibromoanthraquinone, 28 g of dodecylamine, 0.4 g of copper acetate, 5 g of potassium acetate and 40 g of pyridine and the reaction was effected at an elevated temperature of 115°-120° C. for 20 hours under stirring. The reaction product was dissolved in benzene and insoluble matters were separated, followed by distillation of benzene and recrystallization from glacial acetic acid. A blue solid of 1-amino-2,4-di-n-dodecylaminoanthraquinone was obtained by the reaction of the following formula: ##STR8##

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04051052
출처 데이터셋uspto-grants-1977_09
ORD IDord-475519ffedd541a484de268e39aa79e6
출처 메모uspto-grants-1977_09