4-Amino-3,5-xylyl N-methylcarbamate → HCID 53877092, 화합물

HRID 2072438노트

반응식

HRID 2072438 반응식
[CH3:1][NH:2][C:3](=[O:14])[O:4][C:5]1[CH:10]=[C:9]([CH3:11])[C:8]([NH2:12])=[C:7]([CH3:13])[CH:6]=1.[CH2:15]([S:18](Cl)(=[O:20])=[O:19])[CH2:16][CH3:17]>N1C=CC=CC=1>[CH3:1][NH:2][C:3](=[O:14])[O:4][C:5]1[CH:10]=[C:9]([CH3:11])[C:8]([NH:12][S:18]([CH2:15][CH2:16][CH3:17])(=[O:20])=[O:19])=[C:7]([CH3:13])[CH:6]=1

참가 물질

4

반응물 2

HCID 132524-Amino-3,5-xylyl N-methylcarbamateHCID 662791-Propanesulfonyl chloride

생성물 1

HCID 53877092HCID 53877092, 화합물

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

Following the procedure of Example 22, 3,5-dimethyl-4-aminophenyl N-methylcarbamate (0.8g., 0.004 mole) was reacted with n-propanesulfonyl chloride (0.60g., 0.0042 mole) in pyridine. The product (0.8g.) melted at 173°-76° C.

출처 및 근거

ORD 기록
ord-e910ced074ec4eef88f133fc41287ad0
출처 데이터셋
uspto-grants-1977_09
특허 번호
US04051254

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