Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 5-(4-n-Pentylphenyl)-pyrazin-2-yl p-n-propylbenzyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1-(Bromomethyl)-4-propylbenzene | HCID 22246866 | — |
| 반응물 | HCID 178442096 | HCID 178442096 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 5-(4-n-Pentylphenyl)-pyrazin-2-yl p-n-propylbenzyl ether | HCID 19859667 | — |
반응 단계
A mixture of 10.4 g of 5-(4-pentylphenyl)-2-pyrazinol (obtainable analogously to Japanese Preliminary Published Application 144,770/84), 7.7 g of p-n-propylbenzyl bromide, 8.6 g of potassium carbonate and 50 ml of dimethylformamide is heated at 90° for 10 hours. Customary working up gives 5-(4-n-pentylphenyl)-pyrazin-2-yl p-n-propylbenzyl ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04913837 |
| 출처 데이터셋 | uspto-grants-1990_04 |
| ORD ID | ord-7d68e957568f4517a17ac1cc117a670e |
| 출처 메모 | uspto-grants-1990_04 |