Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butyryl chloride → 5-(4'-Pentylbiphenyl-4-yl)-2-propylpyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butyryl chloride | HCID 8855 | — |
| 반응물 | 1-Hexen-3-one | HCID 15395 | — |
| 반응물 | 1,4-Pentadien-3-one | HCID 543199 | — |
| 반응물 | 1-Piperidino-2-(4'-pentylbiphenyl-4-yl)ethene | HCID 54457147 | — |
| 생성물 | 5-(4'-Pentylbiphenyl-4-yl)-2-propylpyridine | HCID 19859150 | — |
반응 단계
Example 11 is repeated by reacting hex-1-en-3-one (preparable starting from butanoyl chloride analogously to the vinyl ketone in Example 11) and 1-piperidino-2-(4'-pentylbiphenyl-4-yl)ethene (preparable analogously to the preparation of the enamine in Example 11) to give 5-(4'-pentylbiphenyl-4-yl)-2-propylpyridine having SE 178° SB 211° SA 222° I.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04913837 |
| 출처 데이터셋 | uspto-grants-1990_04 |
| ORD ID | ord-819764159ce84ba18c8ad3c4d4e277cb |
| 출처 메모 | uspto-grants-1990_04 |