(Dimethyl sulfide)trihydroboron → HCID 19860369, 화합물
반응식
[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]2[O:13][CH2:12][C:11](=O)[N:10]([CH:15]([CH3:17])[CH3:16])[CH2:9]2)[CH:5]=[CH:6][CH:7]=1.B.CSC>CO.C(OCC)(=O)C>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]2[O:13][CH2:12][CH2:11][N:10]([CH:15]([CH3:17])[CH3:16])[CH2:9]2)[CH:5]=[CH:6][CH:7]=1참가 물질
4
실험 절차
The title compound, m.p. 224°-5° C. (methanol-ethyl acetate), was prepared from 2-[3-chlorophenyl]-4-[1-methylethyl]-5-oxomorpholine and borane-methyl sulphide by an analogous procedure to that described in Example 1.
출처 및 근거
- ORD 기록
- ord-8f1f0c7c6fab4a8a893838d2456c707d
- 출처 데이터셋
- uspto-grants-1990_04
- 특허 번호
- US04914202
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