HCID 178433279, 화합물 → HCID 178433265, 화합물

HRID 2072798노트

반응식

HRID 2072798 반응식
[ClH:1].[CH3:2][C:3]1[N:4]=[CH:5][NH:6][C:7]=1[CH2:8]O>S(Cl)(Cl)=O>[ClH:1].[CH3:2][C:3]1[N:4]=[CH:5][NH:6][C:7]=1[CH2:8][Cl:1]

참가 물질

3

반응물 1

HCID 178433279HCID 178433279, 화합물

생성물 1

HCID 178433265HCID 178433265, 화합물

시약·촉매·용매 1

HCID 24386Thionyl Chloride용매

실험 절차

A solution of 10 g of 4-methyl-5-hydroxymethylimidazole hydrochloride in 25 ml of thionyl chloride was allowed to stir at room temperature overnight. The crystalline product was filtered, washed with chloroform and dried, 11 g.

후처리

  1. filtrationThe crystalline product was filtered
  2. washwashed with chloroform
  3. customdried

출처 및 근거

ORD 기록
ord-f61bde152ab046fda9e3187e2ec7263b
출처 데이터셋
uspto-grants-1990_04
특허 번호
US04914207

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