HCID 19855950, 화합물 → HCID 19855928, 화합물

반응식

[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]([CH2:14][N:15]1[CH2:20][CH2:19][N:18]([CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:17][CH2:16]1)[C:12]#[N:13].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]([CH2:14][N:15]1[CH2:20][CH2:19][N:18]([CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:17][CH2:16]1)[CH2:12][NH2:13]

참가 물질

반응물 2

HCID 19855950HCID 19855950, 화합물

HCID 21226445Aluminium lithium hydride

생성물 1

HCID 19855928HCID 19855928, 화합물

실험 절차

In a manner similar to Preparation 2 react α-(2-naphthalenyl)-4-pentylpiperazinepropanenitrile with lithium aluminum hydride to obtain the title compound.

후처리

customIn a manner similar to Preparation 2

출처 및 근거

ORD 기록: ord-a7e2d03e1da549038e875122479f9246
출처 데이터셋: uspto-grants-1990_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04920116

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