HCID 19855933, 화합물 → HCID 19855920, 화합물

반응식

[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[NH:10][C:11](=O)[CH2:12][N:13]([CH2:17][CH:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1)[CH2:14][CH:15]=[CH2:16].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[NH:10][CH2:11][CH2:12][N:13]([CH2:17][CH:18]1[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]1)[CH2:14][CH:15]=[CH2:16]

참가 물질

반응물 2

HCID 19855933HCID 19855933, 화합물

HCID 21226445Aluminium lithium hydride

생성물 1

HCID 19855920HCID 19855920, 화합물

실험 절차

In a manner similar to Preparation 2 react N-(2-chloro-4-methoxyphenyl)-2-[cyclohexylmethyl(2-propenyl)-amino]acetamide with lithium aluminum hydride to obtain the title compound.

후처리

customIn a manner similar to Preparation 2

출처 및 근거

ORD 기록: ord-1dff0a6cd0d043769e44f013c8ff152f
출처 데이터셋: uspto-grants-1990_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04920116

반응 노트

불러오는 중…