Thionyl Chloride → HCID 14368348, 화합물

HRID 2073799노트

반응식

HRID 2073799 반응식
[CH3:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([NH:10][C:11]([NH2:13])=[O:12])[C:3]=1[CH2:4]O.S(Cl)([Cl:16])=O>C(Cl)Cl>[CH3:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([NH:10][C:11]([NH2:13])=[O:12])[C:3]=1[CH2:4][Cl:16]

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 143684562-Methyl-6-ureidobenzyl alcohol

생성물 1

HCID 14368348HCID 14368348, 화합물수율 59.9%

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

A mixture of 2-methyl-6-ureidobenzyl alcohol (1 g) and thionyl chloride (0.66 g) in methylene chloride (20 ml) was stirred for 2 hours at room temperature and evaporated in vacuo. The residue was washed with water and dried in a desiccator to give 2-methyl-6-ureidobenzyl chloride (0.66 g).

후처리

  1. customevaporated in vacuo
  2. washThe residue was washed with water
  3. customdried in a desiccator

출처 및 근거

ORD 기록
ord-48fe8fb720834df79d6fe6d6721b51c3
출처 데이터셋
uspto-grants-1990_04
특허 번호
US04920129

반응 노트

불러오는 중…