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Iodine → HCID 178450060, 화합물

HRID 2074047
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HRID 2074047 반응식
S(=O)(=O)(O)O.[CH2:6]([O:10][C:11]1[CH:20]=[C:19]2[C:14]([CH:15]=[C:16]([CH2:23][CH2:24][C@H:25]3[CH2:30][CH2:29][C@H:28]([CH2:31][CH2:32][CH3:33])[CH2:27][CH2:26]3)[C:17]([F:22])=[C:18]2[F:21])=[CH:13][CH:12]=1)[CH2:7][CH2:8][CH3:9].O.O.[I:36](O)(=O)(=O)=O.II>C(O)(=O)C.O>[CH2:6]([O:10][C:11]1[C:20]([I:36])=[C:19]2[C:14]([CH:15]=[C:16]([CH2:23][CH2:24][C@H:25]3[CH2:30][CH2:29][C@H:28]([CH2:31][CH2:32][CH3:33])[CH2:27][CH2:26]3)[C:17]([F:22])=[C:18]2[F:21])=[CH:13][CH:12]=1)[CH2:7][CH2:8][CH3:9]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

7

반응물 4

HCID 807IodineHCID 1118Sulfuric AcidHCID 86590690HCID 86590690, 화합물HCID 178450059HCID 178450059, 화합물

생성물 1

HCID 178450060HCID 178450060, 화합물수율 378.2%

시약·촉매·용매 2

HCID 176Acetic Acid용매2회
HCID 962
Water
용매
2회

실험 절차

(The following is performed in a draft chamber.) A mixture of concentrated sulfuric acid (1.5 ml), water (10 ml), and glacial acetic acid (50 ml) was dropped for about 10 minutes into a suspension of 7-butoxy-3-[2-(trans-4-propylcyclohexyl)ethyl]-1,2-difluoronaphthalene(21.4 g, 0.053 mol), periodic acid dihydrate (2.6 g, 0.011 mol), and iodine (5.4 g, 0.021 mol) in glacial acetic acid (100 ml) with vigorously stirring. After stirring at 60° C. for 4 hours, the reaction liquid was cooled, poured into water, and the reaction was terminated. The precipitated solid was dissolved with toluene, the organic layer was separated, and was extracted with toluene from the aqueous layer. After collecting organic layers, it was rinsed, in order, with 10% sodium thiosulfate aqueous solution, with saturated sodium hydrogen carbonate aqueous solution, and with saturated brine, and was dried with anhydrous sodium sulfate. A light yellow solid (21.4 g) was obtained by removing the solvent under reduced pressure and by recrystallizing the obtained orange solid (from acetone). (Yield 73.9%)

후처리

  1. stirringAfter stirring at 60° C. for 4 hours
  2. customthe reaction liquid
  3. temperaturewas cooled
  4. customthe reaction was terminated
  5. dissolutionThe precipitated solid was dissolved with toluene
  6. customthe organic layer was separated
  7. extractionwas extracted with toluene from the aqueous layer
  8. customAfter collecting organic layers, it
  9. washwas rinsed, in order, with 10% sodium thiosulfate aqueous solution, with saturated sodium hydrogen carbonate aqueous solution
  10. dry with materialwith saturated brine, and was dried with anhydrous sodium sulfate

출처 및 근거

ORD 기록
ord-d34bca9701f9467f848845fc80319a6c
출처 데이터셋
uspto-grants-2011_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07919154B2

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