Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbamazepine → Carbamazepine p-phthalaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbamazepine | HCID 2554 | — |
| 반응물 | Terephthalaldehyde | HCID 12173 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Carbamazepine p-phthalaldehyde | HCID 131728782 | — |
반응 단계
25 mg (0.1058 mmol) carbamazepine and 7 mg (0.0521 mmol) p-phthalaldehyde were dissolved in approximately 3 mL methanol. Slow evaporation of the solvent yielded colorless needles of a 1:1 carbamazepine/p-phthalaldehyde co-crystal, as shown in FIG. 50A-B.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07927613B2 |
| 출처 데이터셋 | uspto-grants-2011_04 |
| ORD ID | ord-5dfa08e8a2384fe099b1d551c8fdab9f |
| 출처 메모 | uspto-grants-2011_04 |