Benzoyl isothiocyanate → HCID 86625232, 화합물

HRID 2076958노트

반응식

[NH2:1][C:2]1[S:3][C:4]([CH2:10][OH:11])=[C:5]([CH3:9])[C:6]=1[C:7]#[N:8].[C:12]([N:20]=[C:21]=[S:22])(=[O:19])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[C:7]([C:6]1[C:5]([CH3:9])=[C:4]([CH2:10][OH:11])[S:3][C:2]=1[NH:1][C:21]([NH:20][C:12](=[O:19])[C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1)=[S:22])#[N:8]

참가 물질

반응물 2

HCID 68284Benzoyl isothiocyanate

HCID 57456907HCID 57456907, 화합물

생성물 1

HCID 86625232HCID 86625232, 화합물

실험 절차

Prepared as in example 1a from 2-amino-5-(hydroxymethyl)-4-methylthiophene-3-carbonitrile (Example 9b) and benzoyl isothiocyanate as a yellow solid. MS 332 (MH+).

출처 및 근거

ORD 기록: ord-a1241f6cc19843ebaf1e68e712cc54ee
출처 데이터셋: uspto-grants-2011_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07928111B2

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