Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2079496생성일: 2026년 10월 27일
Potassium Carbonate → 4-tert-Butyl-N-[4-chloro-2-(methoxy-pyridin-4-yl-methyl)-Phenyl]-benzenesulfonamide
https://huagongshe.com/reaction/2079496
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-tert-Butyl-N-[4-chloro-2-(chloro-pyridin-4-yl-methyl)-phenyl]-benzenesulfonamide | HCID 59485502 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-tert-Butyl-N-[4-chloro-2-(methoxy-pyridin-4-yl-methyl)-Phenyl]-benzenesulfonamide | HCID 59756865 | — |
반응 단계
A suspension of 4-tert-butyl-N-[4-chloro-2-(chloro-pyridin-4-yl-methyl)-phenyl]-benzenesulfonamide (113 mg, 0.25 mmol) and potassium carbonate (69 mg, 0.5 mmol) in anhydrous methanol was heated at 60° C. overnight, the solid residue was then removed by filtration and product was purified by preparative HPLC. MS: (M+H)=445.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07932252B2 |
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| 출처 데이터셋 | uspto-grants-2011_04 |
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| ORD ID | ord-8243154651194dda942bd5f33ca62a72 |
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| 출처 메모 | uspto-grants-2011_04 |
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