Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(5-Oxiranyl-furan-2-yl)-[1,3]dioxolane → (5-[1,3]Dioxolan-2-yl-furan-2-yl)-acetaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(5-Oxiranyl-furan-2-yl)-[1,3]dioxolane | HCID 23130765 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | (5-[1,3]Dioxolan-2-yl-furan-2-yl)-acetaldehyde | HCID 86042298 | 69.8% |
반응 단계
The resulting 2-(5-oxiranyl-furan-2-yl)-[1,3]dioxolane (2.25 g) and silica gel (5.00 g) were suspended in ethyl acetate (40 mL), and the solution was stirred for 6.5 hours at room temperature. The reaction solution was filtered, then, the filtrate was evaporated in vacuo, and (5-[1,3]dioxolan-2-yl-furan-2-yl)-acetaldehyde (1.57 g) was obtained as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07932272B2 |
| 출처 데이터셋 | uspto-grants-2011_04 |
| ORD ID | ord-e5c89323eebe410eaa5f3bbf613666b1 |
| 출처 메모 | uspto-grants-2011_04 |