Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(2-Methylpropenyl)-benzylamine → 3-Isobutylbenzylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(2-Methylpropenyl)-benzylamine | HCID 23130720 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-Isobutylbenzylamine | HCID 23130553 | 56.6% |
반응 단계
3-(2-Methylpropenyl)-benzylamine described in Preparation Example 137 (100 mg, 0.621 mmol) was dissolved in ethanol (5 mL), 10% palladium-carbon (50% water wet, 20 mg) was added thereto, and the mixture was stirred for 2 hours at room temperature under hydrogen atmosphere. The catalyst was filtered, then, the solvent was evaporated, and the title compound (58 mg, 56.6%) was obtained as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07932272B2 |
| 출처 데이터셋 | uspto-grants-2011_04 |
| ORD ID | ord-f49fab2946984f2d92c5d12888688d44 |
| 출처 메모 | uspto-grants-2011_04 |